Webb11 dec. 2024 · X線回折 (XRD)は、1つの結晶を対象とする場合と結晶を砕いた粉末試料を対象とする場合に大別されます。 後者は粉末X線回折 (PXRD)と呼ばれ、試料の準備や測定が簡便なことから物質・材料研究において広く用いられる一般的な測定手法となっています。 ※2.結晶の対称性 結晶中における原子は空間的に規則的な繰り返しパターンに … Webbobtained by fitting the XRD patterns with the Rietveld method, ranges between 30 and 38 µm. This implies that the synthesized materials are polycrystalline. The amount of the D …
Nitrogenation behavior of Sm-Fe-N-type HDDR powder depending …
Webb1 nov. 2006 · The result shows that when the Sm2Fe17 powders nitrided for 5 hours from 460°C to 510°C, the lattice constant of the alloy and expanding of the crystal cell increased with the increase of... WebbThe Rietveld refinement of XRD patterns reveals that the obtained single phase of the Sm 2Fe 17−xNi x (x = 0, 0.25, 0.35 and 0.5) compounds can be indexed according to the … dashing diva smith street
The Pressure-Composition-Temperature Relation of the Sm2Fe17 …
Webb1 feb. 2013 · The Sm 2 Fe 17 F x2 identified by the XRD pattern corresponded to the phase near the surface of the grains with high fluorine concentration shown in Fig. 1 (3). These results indicate that the following reaction occurred on the surface of the Sm 2 Fe 17 grain: Sm 2 Fe 17 + x 2 XeF 2 = Sm 2 Fe 17 F x + x 2 Xe Webb6 juni 2000 · Isothermal hydrogenation of Sm 2 Fe 17−y Ga y The XRD patterns of the starting powders showed traces of additional phases e.g. SmFe 2, SmFe 3 and α-Fe. GaSm was detected in the powders with the highest Ga-concentration. The content of the additional phases was less than 3 wt%. Webb10 juni 2016 · Methods of measuring “perfection” of alignment include examination using magneto-optical Kerr effect and Schulz XRD crystallographic determination.[6,10,18,19] Elemental Substitution Optimal magnetic properties of Sm2Co17 have been achieved using a quinary alloy represented by the formula Sm(Coa Feb Cuc Zrd)z where “z” is somewhat … bitec telford telephone number